Contact:Ìý Ìý Kanchan Dutta
Location:Ìý ÌýLab 5050
Documentation
Features:
1. Gas and Liquid feed system
- 3 Mass flow controller (Voegtlin, Hi-Performance red-y smart series, 0-25 sccm)
- Gases:ÌýCH4, Ar, H2, Air, NH3, CO2 (other gases possible)Ìý
- Liquid: syringe pump and evaporatorÌý
- All 1/8" heated Swagelok pipes
2. Reactor
- Quartz glass (ID 6 mm with 15µ frit)
- Temperature: up to 1100Ìý°C
- Heating Rate: 1 - 25 °C/min
- Pressure: 1 atm
- Catalyst loading (up toÌý0.75 ml, ~ 20 mm bed height)
- K-type in-bed thermocouple for furnace control
- Reactor bypass
- Heating and MFC computer controlled
- reducing, oxidizing, corrosive (NH3), inert gas atmosphere
3. Gas Analysis
- Mass spectrometer (GSD301 or HPR20 R&D)
- GC (SRI 8610C Multiple Gas Analyzer #3)
ÌýPictures: