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FBR-II (fixed bed reactor setup)


Contact:Ìý Ìý Kanchan Dutta

Location:Ìý ÌýLab 5050

Documentation


Features:

1. Gas and Liquid feed system

  • 3 Mass flow controller (Voegtlin, Hi-Performance red-y smart series, 0-25 sccm)
  • Gases:ÌýCH4, Ar, H2, Air, NH3, CO2 (other gases possible)Ìý
  • Liquid: syringe pump and evaporatorÌý
  • All 1/8" heated Swagelok pipes

2. Reactor

  • Quartz glass (ID 6 mm with 15µ frit)
  • Temperature: up to 1100Ìý°C
  • Heating Rate: 1 - 25 °C/min
  • Pressure: 1 atm
  • Catalyst loading (up toÌý0.75 ml, ~ 20 mm bed height)
  • K-type in-bed thermocouple for furnace control
  • Reactor bypass
  • Heating and MFC computer controlled
  • reducing, oxidizing, corrosive (NH3), inert gas atmosphere

3. Gas Analysis

  • Mass spectrometer (GSD301 or HPR20 R&D)
  • GC (SRI 8610C Multiple Gas Analyzer #3)

ÌýPictures:

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